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A Beginner’s Guide to Distilling Essential Oils at Home

Humans have a long history with essential oils. Used in cooking, medicine, health and wellness, and beauty for centuries, the distilled liquids of plant materials came to be called “essential oils” during the Renaissance. Theorists at that time believed they were the very essence or spirit of the plant at its most refined.

Where do essential oils come from?

Although some essences and essential oils are created from animal products, such as ambergris or musk, plants are far more productive and varied. Most essential oils are derived of plant materials.

All plants naturally produce between 30 and 100 unique chemical combinations, which gives each plant its individual aroma and flavor. These chemicals can be removed from the plants and the “essence” of that plant captured in an oil, giving its user a heightened experience of the plant’s chemicals. In other words, oil of rose is the rosiness of hundreds of roses in a single bottle; it is rosier than roses.

Plants’ essential oils are harvested through three methods: distillation, expression, and extraction. Distillation of essential oils typically refers to steam distillation.

Sometimes, one plant’s various parts (leaves, stems, flowers, fruits, roots, and bark) can be harvested in each of these three ways to make multiple essential oils. Often, steam distillation cannot be used on delicate plants that cannot withstand the heat.

It is important to always research for the oil you plan to make. You want to make sure you have the right kind of still, the right materials, and are using the part of the plant that will produce the essential oil you want.

What are essential oils used for?

As far back as the ancient Egyptian Queen Cleopatra, people have been using essential oils when cooking, in cosmetics, and in medicines. Recently, they’ve become popular in aromatherapy and homeopathic remedies as well.

Many essential oils have antibacterial or antifungal properties, which could be part of the plant’s own defense mechanism. Research over the last few decades shows an increase in the knowledge and use of essential oils to relieve gastrointestinal issues, skin disorders, and stress.

You can find essential oils used in beauty products, household cleaners, perfumes, candles, foods, and almost anything that has a scent.

Why distill your own essential oils?

If you have an ongoing condition or use a great deal of essential oil on a regular basis, you may find that it becomes expensive very quickly. Depending on the oil, it can cost you hundreds of dollars per gallon. It may be well worth it to purchase a still and make your own oils at home. If you can grow your own herbs and plants used in the distillation, you may save even more.

How to distill your own essential oils

#1: Get a copper still

Copper is widely recognized as the best material for distilling. It has natural antibacterial properties and helps filter impurities out of your final product (the “distillate.”) Copper ions bind with elements like sulfur, which affect your distillate. If you’re distilling essential oils, this is important because it means you will achieve the purest scent of the plant in your oil. Copper also has the most even heating temperature and is very easy to clean.

If you plan to distill water or alcohol in addition to essential oils, you want to consider two separate stills for these products, so the scent or flavor of one does not contaminate the other. Or, consider a flip top column still that is designed to allow you the versatility to make any of them. 

#2: Get your plants

Growing your own plants gives you maximum control over their quality and harvest. Plants harvested at the right time produce the best oils. If purchasing plants, choose the healthiest you can find, especially those grown organically without pesticides, if possible. You need a lot of plant material for a little oil, so buy as much high quality material as you can.

#3: Prepare your plants

Depending on the oil you are creating, you may or may not need to wash the plants first. Some essential oil recipes call for using dried plants, so you may need to dry your plant materials first. However, drying them can reduce the essential oils, and it can be very easy to over-dry plants. Never try to re-moisten them after drying, and never use powdered plant materials or plants you don’t dry yourself. Research how to prepare the plants for the specific essential oils you want to make.

#4: Prepare your equipment

Thoroughly clean and decontaminate all the parts of your still and the containers for the essential oils. Have a clean funnel and several cheesecloths on hand as well, for separating oils from the hydrosol.

#5: Distill your oils

Always distill outdoors or in a well-ventilated area, and have gloves, eye-protection, and a fire extinguisher handy.

Place your still over the heat source, but do not begin heating yet. Using filtered or distilled water, fill your still’s pot to the recommended capacity for the oil you’re producing. Generally between 35% and 50%. Secure the column on the top of the pot, and pack your plant material into the column. Do not be shy about how much you use, and do not be surprised if a run of some essential oils yields as little as 1 millimeter of oil in your collection platform.

When you can fit no more plant material in the column, secure the onion bulb at the top of the column and attach the condenser coil. Don’t forget to set up a collection cup of metal, glass, or high-temperature cookware. Never use plastic to collect material from a heated still.

Prepare a cooling process for the condenser coil using ice packs or cold flowing water. Begin to cool the condenser as you simultaneously heat the pot to boiling. When 1-2 drops per second are flowing from the condenser into the collection cup, lower the heat to continue the flow at that rate. When no more hydrosol is being collected, you can turn off the heat. Allow all parts of the still to cool before disassembling it to collect your oils and clean the still.

#6: Collect your essential oil and hydrosol

Different types of column stills will allow you to empty your essential oil from the still in different ways. Make sure you read the owners recommendations for the still you purchase. You should be able to simply filter the hydrosol from the collection cup through a clean cheesecloth before using a clean funnel to funnel it into its final containers.

It can take a huge amount of plant material to harvest a substantial amount of essential oil. Don’t be surprised if you have as little as 1 millimeter of oil after a single run.

#7: Preserve, Store, and Enjoy

Store essential oils in stainless steel or dark glass containers for the best results. Store them away from direct sunlight, and make sure to use a cork or a screw-cap to prevent them from evaporating. Some essential oils lose potency very quickly in open air.

While most essential oils can last for more than two years, they are concentrated and can use some dilution to achieve their ideal effect. Combine your essential oil with a carrier oil like grape seed or almond oil to increase its shelf-life and prevent it from being overpowering.

 

While many essential oils have been synthesized, there may be nothing quite like the natural oils, depending on your purpose for them. To scent perfume or other beauty products, synthetics will do nicely, however for cooking, healthcare, or true aromatherapy, the best results come from natural essential oils. And if you’re using essential oils often and want the best, there’s nothing like making them yourself.

Article by: Jim Thomas

 

Photo credit: "Rose Noblesse" by T. Kiya

Photo credit: "Antique glass bottles" by Nancy

April 14, 2015

Posted in column still, flip top still, pot still


Pot Still vs Flip Top Still

What type of still should I use?

Distilling separates different plant materials using heat, water, and steam. It is a process of steaming what you want to distill, then cooling that steam back into a liquid and condensing it into a container. Distilling has been used throughout the centuries to purify water, to make different alcohols, and to refine plants for their essential oils. Because it is a process that has many uses, different types of stills have been developed to tackle these tasks.

Today, two of the most common still types are the pot still and the flip top column still.

What is the difference between a pot still and a flip top column still?

In short, the difference is the method with which each still uses steam to remove the desired material (the “distillate”) from the plants.

In a pot still the materials are placed directly in the water, which is boiled. The distillate travels with the steam, through the coil, and into the collection cup. This is the method of distilling usually used to make water and alcohols, although some types of essential oil are produced this way.

In a flip top column still the materials are placed in the column above the boiling water. As steam passes through the plants, they drip the distillate into the perforated platforms that attach to the column’s interior. At the top of the column, the steam condenses down the coil and into a collection cup. This is the method of distilling usually used to make essential oils and hydrosols - or “essence waters,” like “rose water” or “lavender water.”

The design of the flip top still makes it usable with the column attached to the pot and the onion head, or with the column rotated on the hinge so it is out of the way, and the onion head attached directly to the pot. Although this can make the flip top more versatile, it is also additional pieces to clean and maintain.

#1: The Pot Still

A pot still can be made of several different materials, but the best is a copper pot still. Because copper has antibacterial and antifungal properties, it will help to purify whatever you’re distilling - whether essential oils, alcohol, or water.

Parts of the still

The pot: A solid, round, enclosed tub which is placed over the heat source

The onion head: The narrowing bulb at the top of the pot, which resembles an onion

The condenser coil: The long copper tubing that attaches at the top of the onion head and slopes downward to an open spout

The collection cup: The container you place under the spout to catch your distillation. You can use metal, glass, or certain pottery, but you should never use plastic to collect distilled materials.


How to use a pot still

After thoroughly cleaning the parts of the copper still, you will place the pot over your heat source. (Always distill alcohol outdoors or in a well-ventilated area). You will pour the water, alcohol mash, or combination of water and plant materials into the pot. Assemble the onion head and condenser coil in place, sealing them with a flour paste mixture. Set up your cooling system for your condenser coil and get your collection cup in place. Turn on the heat and begin your distillation run. When the run is over, turn off the heat and allow all parts of the still to cool before disassembling and cleaning.


#2: The Flip Top Still

A flip top still can be made of several materials, but the best is copper. Because flip top stills are often used for essential oil distillation, the scent of the still’s material can be very important. Stainless steel stills may trap certain toxins and hold scents that taint the final essential oil. However, copper has antibacterial and antifungal properties, so it will help to purify the scents of the essential oils.

Parts of the still

The pot: A solid, round, enclosed tub which is placed over the heat source

The column: A cylindrical tube that is fixed to the top of the pot with an attached hinge. The top attaches to the onion head. Inside the column will be one or two levels of sieves, and one or two platforms with perforated holes, which allow steam to rise through the plants and the oil to drip down and collect on the platforms.

The onion head: The narrowing bulb at the top of the pot, which resembles an onion.

The condenser coil: The long copper tubing that attaches at the top of the onion head and slopes downward to an open spout.

The collection cup: The container you place under the spout to catch your distillation. You can use metal, glass, or certain pottery, but you should never use plastic to collect distilled materials.

How to use a flip top still

Thoroughly clean the parts of your copper flip top still, then set the pot over your heat source. (Consider distilling outside or in a well ventilated area for safety). Fill the pot 35-50% with water, and put the column in place. Pack your plant materials into the sieve or top platform, and don’t be shy about getting as much of it in there as you can.

Attach the onion top and condenser coil and seal the seams with a homemade flour paste, if necessary. Set up the cooling system for your condenser coil and put your steam-collection cup in place. This distilled, essence-infused steam becomes the hydrosol. Turn on your heat and begin your run. When the run is over, cut the heat and leave all copper still parts to cool before disassembling, collecting your oil, and cleaning.

Which still is better: pot still or flip top column still?

There is no real answer here - it depends on what you want to distill. If you think you will need a column occasionally but will use a pot still design most of the time, the flip top still design gives you that versatility. However, if you plan to only distill liquids that can be distilled in pot stills, the column on a flip top may just be unnecessary.

Whether you’re making spirits, purifying water, or creating essential oils, you should choose a copper still that suits your needs.

 

Article by: Jim Thomas

How to Clean a Copper Still Inside and Out

5 gallon copper still assembled

Copper is a durable, rich material that will last you decades if cleaned and cared for properly. It’s inexpensive to clean your copper still, but it does take a little time and effort on a regular schedule to keep it in tip-top, polished condition. You can clean your copper still with homemade recipes of flour, vinegar, and salt, or you can purchase commercial copper cleaners. Using a commercial cleaner may require additional steps or safety precautions before using the still for a run.

What if I don’t clean my copper still?

Copper reacts to oxygen over time (it “oxidizes”), developing a dark brown and then a green lustre if not regularly cleaned. Think of the color of a 20-year-old penny or the Statue of Liberty - that is what happens to unpolished copper.

This coloration is called a “patina,” and some people prefer the natural copper look for their stills. You can own a perfectly useable copper still and let the outside develop its natural patina. However, to keep the interior safe to produce useable distillates (such as alcohol that’s safe to drink and essential oils that are free of toxins), you will want to thoroughly clean the interior of your still after each use.

The first cleaning and vinegar run

When you are ready to use your copper still for the first time, gather the disassembled parts and wash them thoroughly with hot, soapy water. After drying them, you will perform a “vinegar run” to remove impurities and prep the still for use.

Place the pot of your still over your heat source, and fill it to about 20% capacity with an equal mixture of water and vinegar. Assemble the parts of the still and turn on the heat without setting up your cooling process for the condenser. Soon after the water boils, steam, water, and vinegar will come out of the condenser spout into your collection container. You can turn off the heat, and you should allow all parts of the copper still to cool before disassembling, rinsing with hot water, drying, and using them for the first run of your distilled water, alcohol, or essential oil.


Regular interior maintenance

If you’re using your copper still, it’s important for the safety and purity of your products that you keep the interior clean. In addition to the important vinegar run before the first use, you will want to let your still cool thoroughly and disassemble it for cleaning after every use. The heat and alcohol vapors help protect and clean the copper, but you want to make sure that no build up collects which could contaminate your alcohol or essential oils.

After rinsing your copper still pot, fill it to about 10% capacity with clean water and dedicate an unused toilet scrub brush as your still-cleaning brush. Scrub all parts of the pot’s interior thoroughly. If your copper still has a column, rinse it well, and then use a carboy cleaning brush to scrub it - it should be about the right size and shape for the job. Rinse your copper still thoroughly with clean water, and dry it completely. Store it in a safe, dry place until its next use.


Polishing the copper

Spot clean:To spot clean tarnish that begins to appear on the outside of your copper still, you can use ketchup. Simply rub onto the spot, let it sit for 10-15 minutes, and remove thoroughly with a dry cloth. The vinegar in the ketchup will help remove the tarnish efficiently, but the ketchup does leave a slight smell if not thoroughly cleaned off. You could clean your entire copper still with ketchup, but it might cost you a lot of time.


Organic clean: If you want to keep all of your copper still shiny, a combination of flour, vinegar, and salt will give you great results. Calculate the recipe for your still based on its size (5 gallon, 10 gallon, etc). For every gallon, combine 1 tablespoon of salt and 1 cup of vinegar. Then, add flour until the mixture creates a paste. The paste is applied to the copper, left for 30 minutes to dry, and removed. You can repeat the process if necessary.


Commercial products: With very little effort, you can clean your copper thoroughly and keep it looking polished and new with a commercial copper cleaning product. Products like Tarn-X are available at home improvement supply stores, as is the safety equipment you should purchase to use them. (You will want gloves, eye protection, and a mask). These commercial cleaners have strong chemical odors and can leave residues, so they are not recommended for use on the inside of your copper still. You will also want to use commercial cleaners outdoors or in a well-ventilated area, and follow the directions exactly.


Whether your copper still is a decoration or a tool that you utilize, it is a beautiful piece that adds value to your home. Keep it clean and enjoy its beauty as well as its usefulness.


Article by: Jim Thomas